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Front Cover Picture: Two‐Step Continuous‐Flow Synthesis of Fungicide Metalaxyl through Catalytic C−N Bond‐Formation Processes (Adv. Synth. Catal. 1/2022)
The front cover picture, depicts Metalaxyl, an acylalanine fungicide, which was synthesized through catalytic continuous s...
Advanced Synthesis & Catalysis
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Tris(pentafluorophenyl)borane‐Catalyzed Oxygen Insertion Reaction of α‐Diazoesters (α‐Diazoamides) with Dimethyl Sulfoxide
A tris(pentafluorophenyl)borane-catalyzed oxidation reaction of α-diazoesters (α-diazo amides) with dimethyl s...
Advanced Synthesis & Catalysis
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A Synthetic Protocol for the Construction of Chroman‐Spiroquinazolin(thi)one Framework via a Metal‐Free, Three‐Component, Domino, Double Annulations
A three-component domino approach for the synthesis of chroman-spiroquinazolin(thi)ones is described. It involves a conden...
Advanced Synthesis & Catalysis
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Synthesis of SCF3‐Substituted Sulfonium Ylides from Sulfonium Salts or α‐Bromoacetic Esters
A metal-free direct trifluoromethylthiolation of sulfonium ylides with an electrophilic trifluoromethylthiolating reagent ...
Advanced Synthesis & Catalysis
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Electrochemical Ammonium Cation‐Assisted Hydropyridylation of Ketone‐Activated Alkenes: Experimental and Computational Mechanistic Studies
Abstract. This work describes an electrochemical ammonium cation enabled hydropyridylation of ketone-activated alkenes und...
Advanced Synthesis & Catalysis
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Hydrogenation of Esters by Manganese Catalysts
The hydrogenation of esters catalyzed by a manganese complex of phosphine-aminopyridine ligand was developed. Using this p...
Advanced Synthesis & Catalysis
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Synthesis of Enantioenriched Amines by Iron‐Catalysed Amination of Alcohols Employing at Least One Achiral Substrate
Abstract The synthesis of a broad range of enantioenriched amines by the direct Fe-catalysed coupling of amines with alcoh...
Advanced Synthesis & Catalysis
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Front Cover Picture: Synthesis of Enantioenriched Amines by Iron‐Catalysed Amination of Alcohols Employing at Least One Achiral Substrate (Adv. Synth. Catal. 24/2021)
The Front Cover Picture, designed by Anastasiia Afanasenko, illustrates the methodology for the synthesis of enantioenrich...
Advanced Synthesis & Catalysis
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Diastereoselective Bidirectional C(sp3)‐H Bond Functionalization of Piperazine Compounds
A highly diastereoselective bidirectional C(sp3)-H bond functionalization of piperazine compounds, triggered by a Lewis ac...
Advanced Synthesis & Catalysis
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Electrochemically Mediated Direct C(sp3)‐H Sulfonylation of Xanthene Derivatives
The construction of C(sp3)-sulfonyl bonds through direct sulfonylation of C(sp3)-H bond presents a number of challenges, s...
Advanced Synthesis & Catalysis
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Stereoselective Cyclopropanation of Boron Dipyrromethene (BODIPY) Derivatives by an Organocascade Reaction
Abstract The synthesis of enantiopure chiral boron dipyrromethenes (BODIPYs) is of importance due the intrinsic properties...
Advanced Synthesis & Catalysis
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Rhodium(III)‐Catalyzed Aldehyde C‐H Activation and Functionalization with Dioxazolones: An Entry to Imide Synthesis
A rhodium(III)-based catalytic system has been used to develop a C-H bond activation of benzaldehyde derivatives and subse...
Advanced Synthesis & Catalysis
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Ruthenium‐Catalyzed Vinylene Carbonate Annulation by C–H/N–H Functionalizations: Step‐Economical Access to Indoles
A convenient and effective method of ruthenium-catalyzed C–H/N–H annulations using vinylene carbonate as oxi...
Advanced Synthesis & Catalysis
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Pd‐Catalyzed Atropselective C‐H Olefination Promoted by a Transient Directing Group
A Pd(II)-catalyzed atroposelective olefination of biaryls with maleimides is reported using chiral transient directing gro...
Advanced Synthesis & Catalysis
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Visible‐Light‐Assisted Synthesis of Allylic Triflamides via Dual Acridinium/Co Catalysis
An efficient dehydrogenative functionalization of styryl carbon-carbon double bonds with triflamide is described via dual ...
Advanced Synthesis & Catalysis
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BiCl3‐Mediated Tandem Cyclization of Tryptamine‐Derived Ynamide: Concise Synthesis of Pentacyclic Spiroindolines and Tricyclic Indole Derivatives
Catalytic tandem cyclization of ynamides has attracted considerable interest in organic synthesis because of its atom econ...
Advanced Synthesis & Catalysis
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Palladium‐Catalyzed Carbamoyl‐Carbamoylation/ Carboxylation/Thioesterification of Alkene‐Tethered Carbamoyl Chlorides using Mo(CO)6 as the Carbonyl Source
We reported a palladium-catalyzed carbamoyl-carbamoylation/carboxylation/thioesterification of alkene-tethered carbamoyl c...
Advanced Synthesis & Catalysis
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Asymmetric Synthesis of Chiral α‐CF2H spiro[indoline‐3,3'‐thiophene] via Phase‐Transfer Catalyzed Sulfa‐Michael/Michael Domino Reaction
Abstract. An efficient and practical sulfa-Michael/Michael domino reaction of (E)-4-mercapto-2-butenoates with difluoromet...
Advanced Synthesis & Catalysis
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Minisci‐type Alkylation of N‐Heteroarenes by N‐(Acyloxy)phthalimides Mediated by a Hantzsch Ester and Blue LED Light
A synthetic method that enables the Hantzsch ester-mediated Minisci-type C2-alkylation of quinolines, isoquinolines and py...
Advanced Synthesis & Catalysis
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H2O2‐Mediated Synthesis of 1,2,4‐Thiadiazole Derivatives in Ethanol at Room Temperature
Herein, we report the H2O2-mediated synthesis of 1,2,4-thiadiazole derivatives under metal-free conditions at room tempera...
Advanced Synthesis & Catalysis
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Iron‐Catalyzed One‐step Synthesis of Isothiazolone/1,2‐Selenazolone Derivatives via [3+1+1] Annulation of Cyclopropenones, Anilines, and Elemental Chalcogens
Described herein is the one-step synthesis of isothiazolone/1,2-selenazolone derivatives via [3+1+1] cycloaddition of cycl...
Advanced Synthesis & Catalysis
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Nickel‐Catalyzed Decarbonylative Cycloaddition of Benzofuran‐2,3‐diones with Alkynes to Flavones
Using dppe as the ligand, the Nickel-catalyzed decarbonylative cycloaddition of benzofuran-2,3-diones with alkynes was est...
Advanced Synthesis & Catalysis
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Rhodium‐Catalysed Asymmetric Arylation of Pyridylimines
The catalytic asymmetric arylation of pyridylimines was developed. A range of pyridylimines reacted with arylboronic acids...
Advanced Synthesis & Catalysis
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Front Cover Picture: Lewis Acid‐Catalyzed Formal (4+2)‐ and (2+2+2)‐Cycloaddition Between 1‐Azadienes and Styrylmalonates as Analogues of Donor‐Acceptor Cyclopropanes (Adv. Synth. Catal. 23/2021)
The front cover picture, designed by Pavel G. Sergeev and Daria I. Filina, illustrates the comparison between reactivities...
Advanced Synthesis & Catalysis
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Acridine Orange Hemi(Zinc Chloride) Salt as a Lewis Acid‐Photoredox Hybrid Catalyst for the Generation of α‐Carbonyl Radicals
Abstract A readily accessible organic-inorganic hybrid catalyst is reported for the reductive fragmentation of α-hal...
Advanced Synthesis & Catalysis
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The regioselective Arylation of 1,3‐Benzodioxoles
The direct arylation of 1,3-benzodioxole and 2,2-difluorobenzo[1,3]dioxole with 28 different aryl bromides yields the resp...
Advanced Synthesis & Catalysis
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Combined Photoredox and Carbene Catalysis for the Synthesis of γ‐Aryloxy Ketones
N-heterocyclic carbenes (NHCs) have emerged as catalysts for the construction of C–C bonds in the synthesis of subs...
Advanced Synthesis & Catalysis
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Calcium‐Catalyzed Intramolecular Hydroamination‐Deacylation Reaction of in situ formed β‐Amino Allenes
We have developed a simple, One-Pot, three-component reaction of tert-propargyl alcohols, primary amines and acyl ketones ...
Advanced Synthesis & Catalysis
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Synthesis of Substituted 1‐Hydroxy‐2‐naphthaldehydes by Rhodium‐Catalyzed C‒H Bond Activation and Vinylene Transfer of Enaminones with Vinylene Carbonate
The rhodium(III)-catalyzed C‒H bond activation and vinylene transfer of enaminones with vinylene carbonate have bee...
Advanced Synthesis & Catalysis
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Gold(I)‐Catalyzed Selective Cyclization and 1,2‐Shift to Prepare Pseudorutaecarpine Derivatives
A variety of pseudorutaecarpine derivatives were prepared in good to excellent yields through a gold(I)-catalyzed selectiv...
Advanced Synthesis & Catalysis
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