Accurate Quantification of Pure Thiacloprid with Mass Balance and Quantitative H-NMR

Jeschke P, Moriya K. Five-membered neonicotinoids: imidacloprid and thiacloprid. In: Jeschke P, Witschel M, Krämer W, editors. Modern crop protection compounds. 3rd ed. Weinheim: Wiley-VCH Verlag GmbH & Co. KGaA; 2019. p. 1293–308.

Chapter  Google Scholar 

Akram S, Sultana B, Asi MR, Mushtaq M. Salting-out-assisted liquid–liquid extraction and reverse-phase high-performance liquid chromatographic monitoring of thiacloprid in fruits and vegetables. Sep Sci Technol. 2018;53(10):1563–71.

Article  CAS  Google Scholar 

Angioni A, Porcu L, Pirisi F. LC/DAD/ESI/MS method for the determination of imidacloprid, thiacloprid, and spinosad in olives and olive oil after field treatment. J Agric Food Chem. 2011;59(20):11359–66.

Article  CAS  PubMed  Google Scholar 

Mitchell EAD, Mulhauser B, Mulot M, Mutabazi A, Glauser G, Aebi A. A worldwide survey of neonicotinoids in honey. Science. 2017;358(6359):109–11.

Article  CAS  PubMed  Google Scholar 

Ma W, Yang B, Li J, Li X. Amino-functional metal-organic framework as a general applicable adsorbent for simultaneous enrichment of nine neonicotinoids. Chem Eng J. 2022;434: 134629.

Article  CAS  Google Scholar 

Yang B, Ma W, Wang S, Shi L, Li X, Ma Z, Zhang Q, Li H. Determination of eight neonicotinoid insecticides in Chinese cabbage using a modified QuEChERS method combined with ultra performance liquid chromatography-tandem mass spectrometry. Food Chem. 2022;387: 132935.

Article  CAS  PubMed  Google Scholar 

Rundlöf M, Andersson GKS, Bommarco R, Fries I, Hederström V, Herbertsson L, Jonsson O, Klatt BK, Pedersen TR, Yourstone J, Smith HG. Seed coating with a neonicotinoid insecticide negatively affects wild bees. Nature. 2015;521(7550):77–80.

Article  PubMed  Google Scholar 

Yamamuro M, Komuro T, Kamiya H, Kato T, Hasegawa H, Kameda Y. Neonicotinoids disrupt aquatic food webs and decrease fishery yields. Science. 2019;366(6465):620–3.

Article  CAS  PubMed  Google Scholar 

Cimino AM, Boyles AL, Thayer KA, Perry MJ. Effects of neonicotinoid pesticide exposure on human health: a systematic review. Environ Health Persp. 2017;125(2):155–62.

Article  CAS  Google Scholar 

Dupraz-Dobias P. France bans all uses of neonicotinoid pesticides. In: Chemical&Engineering News. American Chemical Society. 2018. https://cen.acs.org/environment/pesticides/France-bans-uses-neonicotinoid-pesticides/96/i36. Accessed 5 Nov 2023.

Carbonell-Rozas L, Lara FJ, Del Olmo IM, Garcia-Campana AM. Micellar electrokinetic chromatography as efficient alternative for the multiresidue determination of seven neonicotinoids and 6-chloronicotinic acid in environmental samples. Anal Bioanal Chem. 2019;412(24):6231–40.

Article  PubMed  Google Scholar 

Zhang J, Yang R, Zhou X, Wang Y. Advances in analytical methods of neonicotinoid insecticides. Chin J Anal Lab. 2023;42(7):974–83.

CAS  Google Scholar 

Wang X, Zhang W, Wang M, Ma Y, Han Y, Deng B, Gao M, Tong J, Shen S, Feng D. Simultaneous determination of ten neonicotinoid pesticides in vegetables by dispersed solid-phase extraction coupled with ultra performance liquid chromatography-tandem mass spectrometry. Chin J Anal Lab. 2023;42(7):897–902.

CAS  Google Scholar 

Abdulhussein AQ, Jamil AKM, Bakar NKA. Magnetic molecularly imprinted polymer nanoparticles for the extraction and clean-up of thiamethoxam and thiacloprid in light and dark honey. Food Chem. 2021;359:129936.

Article  CAS  PubMed  Google Scholar 

Martínez-Pérez-Cejuela H, Pravcová K, Česlová L, Simó-Alfonso EF, Herrero-Martínez JM. Zeolitic imidazolate framework-8 decorated with gold nanoparticles for solid-phase extraction of neonicotinoids in agricultural samples. Microchim Acta. 2021;188(6):197.

Article  Google Scholar 

Westwood S, Choteau T, Daireaux A, Josephs RD, Wielgosz RI. Mass balance method for the SI value assignment of the purity of organic compounds. Anal Chem. 2013;85(6):3118–26.

Article  CAS  PubMed  Google Scholar 

Mahajan S, Singh IP. Determining and reporting purity of organic molecules: why qNMR. Magn Reson Chem. 2013;51(2):76–81.

Article  CAS  PubMed  Google Scholar 

Nelson MA, Bedner M, Lang BE, Toman B, Lippa KA. Metrological approaches to organic chemical purity: primary reference materials for vitamin D metabolites. Anal Bioanal Chem. 2015;407(28):8557–69.

Article  CAS  PubMed  Google Scholar 

Yang M, Wang M, Zhou J, Song Y, Wang T. Development of a new certified reference material of tinidazole for quality and safety of agro-products. Accredit Qual Assur. 2016;21(5):341–9.

Article  Google Scholar 

Maienfisch P. Challenges and risks associated with impurity profiles in technical grade crop protection products produced semi-synthetically from natural products. Adv Agrochem. 2022;1(2):148–56.

Article  Google Scholar 

Li X, Tu M, Yang B, Ma W, Li H. Structurally related impurity profiling of thiacloprid by orbitrap and de novo identification tool. Microchem J. 2023;193: 109123.

Article  CAS  Google Scholar 

State Admimistration for Market Regulation. JJF 1855–2020. Metrological technical specification for purity assessment of certified reference materials-organic purity certified reference materials. Beijing: Standards Press of China; 2020. http://jjg.spc.org.cn/resmea/standard/JJF%25201855-2020/. Accessed 11 Nov 2023.

Li X, Ma W, Yang B, Tu M, Zhang Q, Li H. Impurity profiling of dinotefuran by high resolution mass spectrometry and SIRIUS tool. Molecules. 2022;27(16):5251.

Article  CAS  PubMed  PubMed Central  Google Scholar 

Li X, Li H, Zhang W, Li X, Zhang Q, Guo Z, Li X, Song S, Zhao G. Development of patulin certified reference material using mass balance and quantitative NMR. World Mycotoxin J. 2021;15(2):135–42.

Article  Google Scholar 

Li X, Zhang W, Zhou S, Li X, Tu M, Zhu Y, Zhang Q, Li H. Purity assessment of thiamethoxam using mass balance and quantitative nuclear magnetic resonance. Microchem J. 2023;191: 108874.

Article  CAS  Google Scholar 

Li X, Zhang W, Li X, Zhou S, Tu M, Zhu Y, Li H. Purity assessment of dinotefuran using mass balance and quantitative nuclear magnetic resonance. Molecules. 2023;28(9):3884.

Article  CAS  PubMed  PubMed Central  Google Scholar 

Jiang Y, Huang X, Wang X, Zhang Y. Insecticedes. In: Pesticide Analysis Manual. 1st ed. Beijing: Chemical Industry Press; 2012. pp. 202–205.

KKNW. Thiacloprid; LC-ESI-QQ; MS2; CE:20 V; [M+H]+. In: MassBank. 2016. https://massbank.eu/MassBank/RecordDisplay?id=MSBNK-Waters-WA000082&dsn=Waters. Accessed 11 Nov 2023.

Chen J, Zhao X, Zhang Z, Chen Y, Fu X, Liu Y. Separation and characterization of the impurities in 3,3-diamino-4,4-azoxyfurazan by ultrahigh-performance liquid chromatography combined with Qorbitrap mass spectrometry. Microchem J. 2021;170: 106647.

Article  CAS  Google Scholar 

Kozo S, Shinichi T, Shinzo K, Shoko S, Koichi M, Yumi H. Heterocyclic compounds. US-4849432-A, 7/17641. 1989. https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/4849432. Accessed 11 Sep 2020

Lippa KA, Duewer DL, Nelson MA, Davies SR, Mackay LG. The role of the CCQM OAWG in providing SI traceable calibrators for organic chemical measurements. Accred Qual Assur. 2019;24(6):407–15.

Article  CAS  Google Scholar 

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