Solvation role of dimethyl sulfoxide on the interaction with dentin bonding systems after 30 months

Elsevier

Available online 16 March 2023

Dental MaterialsAuthor links open overlay panel, , , , , Highlights•

DMSO appears to be a promising agent to increase the bond strength to dentin.

DMSO was able to increase the degree of conversion of non-simplified adhesive systems.

For etch-and-rinse and universal adhesive systems, the dentin pretreatment with DMSO enhanced the resin-dentin interface.

AbstractObjectives

To determine whether DMSO could serve as an effective pretreatment to improve the mechanical properties and minimize the degradation of the adhesive interface, through the degree of conversion (DC) and bond strength to dentin of different categories of dentin bonding systems (DBSs) after 30 months.

Methods

DMSO (0, 0.5, 1, 2, 5, 10 vol%) were incorporated into four categories of DBSs: Adper Scotchbond Multipurpose (MP), Adper Single Bond 2 (SB), Clearfil SE Bond (CSE) and Adper Scotchbond Universal (SU). DC was evaluated by Fourier transform infrared spectroscopy (FTIR). For microtensile bond strength test (µTBS), 1 % DMSO were applied on dentin as pretreatment before DBSs. For SU, both strategies were tested. Specimens for µTBS were tested after 24 h, 6 and 30 months. DC and µTBS data were subjected to two-way ANOVA and Tukey test (α < 0.05).

Results

Incorporating 5 %/10 % DMSO increased the DC of CSE. Controversially, when combined with SU, 2 % and 10 % DMSO jeopardized the DC. Regarding µTBS, 1 % DMSO pre-treatment increased the bond strength for MP, SB, SU-ER and SU-SE. After 30 months, MP, SU-ER and SU-SE showed a decrease compared to baseline but remained higher than the control.

Clinical significance

DMSO pretreatment may be a useful strategy to improve the bond interface over time. Its incorporation seems to favor the non-solvated systems regarding DC while it seems to show long-term benefits for bond strength using 1 % DMSO for MP and SU systems.

Keywords

Adhesion

Dentin

Dimethyl sulfoxide

Micro-tensile

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© 2023 The Academy of Dental Materials. Published by Elsevier Inc. All rights reserved.

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