Available online 17 November 2022
Highlights•Radiant heat treatment with a diode laser (445 nm) was tested for thermo-curing of GICs.
•Four conventional GICs were tested and setting process was monitored by FTIR.
•A LED device was used for comparison with the diode laser irradiating at the same fluence.
•Both treatments were beneficial for the progress of the setting reaction of GICs.
•Diode laser (445 nm) could be used as alternative light source for thermocuring of conventional GICs.
AbstractObjectivesThe aim of this study was to investigate the effect of thermal energy induced by a diode laser (445 nm) on the setting reactions of conventional glass ionomer cements (GICs) by using Fourier transform infrared spectroscopy (FTIR) and to compare it with that induced by a LED device.
MethodsFour GICs were investigated in this study (GlassIonomer FX Ultra, Ketac Universal Aplicap, Equia Fill, and Riva Self Cure). The experimental groups of the study were as follows (n = 5): Group 1 (control) – the specimens after mixing were left to set without any treatment; Group 2 – the specimens were irradiated for 60 s using a LED (Valo™) at 1400 mW/cm2 (fluence ∼ 1.4 J/cm2); Group 3 – the specimens were also irradiated for 60 s using a diode laser (SIROLaser Blue), which emits at 445 ± 5 nm with average output power of 0.7 W (fluence ∼ 1.4 J/cm2). FTIR analysis of the GIC specimens was followed to assess the changes in the COO-/CO ratios of the setting reaction and its progress in time.
ResultsBoth laser and LED treatments improved the setting reactions of the GICs compared to the control group (p < 0.05). However, this phenomenon was not observed in all materials implying that it may be material dependent.
SignificanceRadiant heat treatments using diode laser or LED may be beneficial for the rate and progress of setting reaction of the conventional GICs. The composition and handling of the materials may be crucial for their final properties and the overall clinical behavior.
KeywordsConventional glass ionomer cements
Diode laser
Fourier transform infrared spectroscopy
Light-emitting diode
Thermo-curing
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