Available online 3 October 2022
Highlights•Depth of cure (DoC) was determined using Knoop microhardness profiles 24 h post cure.
•All tested materials met the manufacturers’ claims for DoC.
•30 d storage in 37 °C water significantly decreased KIC of ion releasing resin based composite.
•Ion releasing resin based composite showed less wear resistance after cyclic loading.
AbstractObjectivesTo investigate the depth of cure (DoC), fracture toughness (KIC) and wear of ion releasing resin-based composite (RBC) restorative materials.
MethodsTwo ion releasing RBCs, Activa (ACT) and Cention-N (CN) were compared to a conventional RBC (Z350) and a resin-modified glass ionomer cement (Fuji-II-LC). The DoC was measured in a 10-mm deep semi-circular metal mold with a 2-mm internal radius (n = 8). The molds were irradiated from one end for 20-s. The Knoop hardness (KH) was measured at 0.5-mm intervals from the surface after the specimens had been stored at 37 °C for 24-h. To measure the KIC, single-edge-notched specimens (n = 15/group) were prepared (25×5x2.5-mm) for a 3-point bending test and then stored for either 1 or 30-days in water at 37 °C. Disk-shaped specimens (n = 10) were subjected to 250,000-load cycles of 49-N using a chewing simulator against spherical steatite antagonists. DoC and wear data were analyzed by one-way ANOVA and Tukey post hoc tests (p ≤ 0.05). KIC data were analyzed by two-way ANOVA and one-way ANOVA, and the Tukey post hoc test (p ≤ 0.05). In addition, an independent t-test was used to determine if storage time had any effect (α = 0.05) on the KIC of each material.
ResultsMaximum hardness value was the highest for Z350 and the lowest for ACT. The depth at which 80% of the maximum KH, was the highest for CN (9.2 mm) and the lowest for Z350 (2 mm). All tested materials met the manufacturers’ claims for DoC. After 1-day, the highest KIC values were recorded for ACT and the lowest for Fuji-II-LC. Water storage (30-days) significantly reduced the KIC value for all materials except Fuji-II-LC. The highest wear rate values were recorded for CN followed by ACT.
SignificanceAll tested materials met their manufacturers’ claims for DoC. Water storage for 30-days significantly reduced the fracture toughness for ACT and CN. Wear was significantly higher for ACT and CN.
KeywordsResin composites
Ion release
Water storage
Depth of cure
Fracture toughness
Wear
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